catalytic hydrogenation in organic syntheses

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Catalytic Hydrogenation In Organic Syntheses

Author : Rylander
ISBN : 9780323138536
Genre : Science
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Catalytic Hydrogenation in Organic Syntheses focuses on the process of catalytic hydrogenation in organic synthesis. This book gives the reader easy access to catalytic history, to show what can be done and how to do it. A variety of working generalities and common sense guides are given as aids in selecting catalytic metal, catalyst support, concentration of metal and catalyst, solvent, and reaction conditions. All manner of hydrogenation catalysts are considered and mechanisms of hydrogenation are presented at a level that is useful to the synthetic organic chemist. This volume is comprised of 15 chapters and begins with an overview of catalytic hydrogenation and heterogeneous hydrogenation catalysts, along with hydrogenation reactors and reaction conditions. The discussion then shifts to the hydrogenation of compounds such as acetylenes, olefins, aldehydes, ketones, nitriles, oximes, acids, esters, lactones, anhydrides, and nitro compounds as well as carbocyclic aromatics and heterocyclic compounds. The reader is also introduced to reductive alkylation, catalytic dehydrohalogenation, and hydrogenolysis of small rings. A chapter on miscellaneous hydrogenolyses concludes the book. This book will be of interest to organic chemists working in the field of catalytic hydrogenation.

Handbook Of Heterogeneous Catalytic Hydrogenation For Organic Synthesis

Author : Shigeo Nishimura
ISBN : 0471396982
Genre : Science
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The most comprehensive reference in the field, Handbook of Heterogeneous Catalytic Hydrogenation for Organic Synthesis provides synthetic chemists and chemical engineers in fine chemicals and pharmaceuticals with detailed experimental guidelines for heterogeneous catalytic hydrogenation. Organized by functional groups for ready reference and featuring detailed examples of hundreds of reactions, this handbook covers hydrogenations of alkenes, alkynes, aldehydes and ketones, nitriles, imines, nitro and nitroso compounds, carboxylic acids and esters, and aromatic and heterocyclic compounds. In addition, coverage includes the preparation of amines by reductive alkylation and the hydrogenolysis of a variety of compounds. Examples of hydrogenation of functional groups and reaction pathways are illustrated with numerous equations and schemes. Practitioners will appreciate the plenitude of experimental details given for most of the reactions selected, including amounts of reagents and catalysts, reaction temperatures, hydrogen pressures, and reaction times. They will also find helpful the more than one hundred tables included throughout the book detailing the effects of key factors governing rate and selectivity, such as compound structure, the nature of catalysts and supports, and the nature of solvents. Researchers will benefit from the introductory chapters covering an array of hydrogenation catalysts, including nickel, cobalt, copper, iron, platinum group metals, rhenium, and other oxide and sulfide catalysts, as well as reactors and reaction conditions.

Catalytic Hydrogenation

Author : Robert L. Augustine
ISBN : UOM:39015028899253
Genre : Catalysis
File Size : 61. 30 MB
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Catalysis In Organic Syntheses

Author : William H. Jones
ISBN : 9781483262048
Genre : Science
File Size : 70. 11 MB
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Catalysis in Organic Syntheses contains the proceedings of the Seventh Conference on Catalysis in Organic Syntheses held in Chicago, 5-7 June 1978. The conference was sponsored by The Organic Reactions Catalysis Society, an affiliate of The Catalysis Society. Most of the papers reflect the main interest of the Society membership, namely, the application of catalysis as a tool for the synthetic organic chemist rather than studies of catalytic phenomena per se, the latter subject being amply covered in other symposia. It is not surprising then that the largest group of papers deal with catalytic hydrogenation, the catalytic reaction most often encountered in organic synthesis. Other subjects in the burgeoning field of catalysis are not neglected however, as evidenced by papers on the spectroscopic evaluation of catalysts, homogenous catalysis by organometallic complexes, and the catalysis of coal conversion. Finally a group of papers explore some safety considerations in performing catalytic transformations.

Innovative Catalysis In Organic Synthesis

Author : Pher G. Andersson
ISBN : 9783527646609
Genre : Science
File Size : 38. 55 MB
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C-H, C-O, C-C, and C-Heteroatom bond forming processes by using metal-ligand approaches for the synthesis of organic compounds of biological, pharmacological and organic nanotechnological utility are the key areas addressed in this book. Authored by a European team of leaders in the field, it brings together innovative approaches for a variety of catalysis reactions and processes frequently applied in organic synthesis into a handy reference work. It covers all major types of catalysis, including homogeneous, heterogeneous, and organocatalysis, as well as mechanistic and computational studies. Special attention is paid to the improvements in efficiency and sustainability of important catalytic processes, such as selective oxidations, hydrogenation, and cross-coupling reactions, and to their utilization in industry. The result is a valuable resource for advanced researchers in both academia and industry, as well as graduate students in organic chemistry aiming for chemo-, regio- or stereoselective synthesis of organic compounds by using novel catalytic systems.

Catalytic Hydrogenation In Organic Synthesis

Author : Morris Freifelder
ISBN : UOM:39015057357983
Genre : Science
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Based on over 22 years of experience, this book presents a substantial accumulation of knowledge. Clearly and understandably written, it gives detailed descriptions of many experiments, providing step-by-step procedures along with personal notes and observations, directions, suggestions, and safety precautions. The yields obtained in these experiments are good to excellent, and most of the hydrogenations discussed are carried out under very mild conditions.

Transition Metal Reagents And Catalysts

Author : Jiro Tsuji
ISBN : 0471560278
Genre : Science
File Size : 77. 53 MB
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Transition Metal Reagents and Catalysts Innovations in Organic Synthesis Jiro Tsuji Emeritus Professor, Tokyo Institute of Technology, Japan Numerous innovative and practical synthetic methods using transition metal complexes as either catalysts or reagents have been developed over the last 35 years. Transition Metal Reagents and Catalysts combines the varied applications of transition metal complexes in a unique and timely book in this rapidly advancing area of organic synthesis. This text is an easily understandable and enjoyable read for organic chemists who are not yet familiar with organo-transition metal chemistry. Transition Metal Reagents and Catalysts presents: * Complete coverage of nearly 35 years of transition metal complex chemistry * An in-depth treatment of many innovative synthetic methodologies * A rational classification of all reactions according to substrates and reaction mechanisms * Examples of important applications of transition metal catalysed reactions. A knowledge of organic synthesis using transition metal complexes is a must for all synthetic organic chemists. Written for chemists who wish to apply novel synthetic methods using transition metal complexes to solve problems in organic and pharmaceutical chemistry, such as synthesis of fine and bulk chemicals and natural products, Transition Metal Reagents and Catalysts is an essential reference source and an indispensible research companion.

Catalysis Of Organic Reactions

Author : John R. Sowa, Jr.
ISBN : 1420028030
Genre : Science
File Size : 41. 62 MB
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This volume compiles 63 peer-reviewed scientific papers documenting the latest developments in the application of homogeneous, heterogeneous, and immobilized homogenous catalysts used in organic synthesis. Catalysis of Organic Reactions consists of primary research articles accompanied by experimental sections that emphasize chemical processes with actual and potential applications in industry. Each chapter represents current and outstanding research by recognized leaders in the field. Organized into five major symposia, topics include selective homogeneous and heterogeneous catalysis for the synthesis of fine chemical and pharmaceuticals, solid acid catalysis, selective oxidation, amination, chiral catalysis, combinatorial technologies, nanoparticles, environmentally friendly catalysis, and more. The collection also presents the award-winning research of Jean Lessard, concerning the scope and limitations of electrocatalytic hydrogenation of organic compounds at Raney Metal Electrodes, and Richard Larock, relating to palladium-catalyzed annulation and migration reactions. These proceedings are of interest to the chemical scientists and engineers whose special interest is to apply homogenous and heterogeneous catalysts in organic synthesis of pharmaceutical, fine, and commodity chemicals.

Advanced Organic Synthesis

Author : Richard Monson
ISBN : 9780323159975
Genre : Science
File Size : 89. 85 MB
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Advanced Organic Synthesis: Methods and Techniques presents a survey and systematic introduction to the modern techniques of organic synthesis. The book attempts to acquaint the reader with a variety of laboratory techniques as well as introduce chemical reagents that require deftness and care in handling. Chapters are devoted that discuss the techniques of organic synthesis; apparatus and terminology used in the description of synthetic procedures; the scope and mechanism of chemical reactions; and technical procedures on how to perform chemical experiments. The text will be of vital importance to advanced undergraduate student or beginning graduate student of chemistry.

Catalytic Hydrogenation

Author : Robert L. Augustine
ISBN : MINN:31951000462864H
Genre : Science
File Size : 48. 99 MB
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