microwave assisted organic synthesis a green chemical approach

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Microwave Assisted Organic Synthesis

Author : Suresh C. Ameta
ISBN : 9781482254242
Genre : Technology & Engineering
File Size : 24. 27 MB
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The large-scale production of chemicals to meet various societal needs has created environmental pollution, including pollution from byproducts and improper disposal of waste. With the world facing adverse consequences due to this pollution, green chemistry is increasingly being viewed as a means to address this concern. Since most organic syntheses require toxic solvents, more reaction time, and drastic conditions of temperature, conventional methods of organic synthesis are less preferred. Microwave-assisted organic synthesis is considered to be a promising green chemical approach because it reduces reaction time from days or hours to minutes or even seconds, and has many other advantages. It helps reduce side reactions and increase yields, uses fewer solvents or is almost solvent-free, has solid supported reactions, and improves purity. This book’s main focus is microwave-assisted organic synthesis processes, particularly various reactions such as cycloaddition, rearrangement, elimination, substitution, oxidation, reduction, condensation, coupling, polymerization, nanomaterials, synthesis of heterocycles, and industrial applications under microwave irradiation. The time is not far off when this methodology will virtually replace existing and cumbersome methods of organic synthesis.

Microwave Assisted Organic Synthesis

Author : D. Bogdal
ISBN : 0080518737
Genre : Science
File Size : 64. 50 MB
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Microwave-assisted Organic Synthesis: One Hundred Reaction Procedures provides readers with a broad overview of microwave assisted Organic Synthesis, enabling students and researchers alike to produce more efficient and high yield syntheses while saving time and resources. The work addresses key problems faced by chemistry laboratories in academia and in industry, that of an ever increasing need for procedures which are low-waste, energy efficient, high yield, occur over a short reaction period, and use environmentally friendly solvents. All these factors play an important role in the development of Green Chemistry methods, and in this, Microwave-assisted Organic Synthesis: One Hundred Reaction Procedures is an excellent resource for any library. Provides a broad overview of microwave enhanced chemistry Extensive references to the source of each procedure, including equipment used, full operating procedure, and associated hazards Includes exercises and worked problems which can support more independent study

Microwave Assisted Organic Synthesis

Author : Jason Tierney
ISBN : 9781405168441
Genre : Science
File Size : 89. 75 MB
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The first reports on the application of microwaves in organicsynthesis date back to 1986, but it was not until the recentintroduction of specifically designed and constructed equipment,which countered the safety and reproducibility concerns, thatsynthetic application of microwaves has become established as alaboratory technique. Microwave assisted synthesis is now beingadopted in many industrial and academic laboratories to takeadvantage of the novel chemistry that can be carried out using avariety of organic reaction types. This book demonstrates the underlying principles of microwavedielectric heating and, by reference to a range of organic reactiontypes, it's effective use in synthetic organic chemistry. Toillustrate the impact microwave assisted organic synthesis can haveon chemical research, case studies drawn mainly from thepharmaceutical industry are presented.

Microwave Chemical And Materials Processing

Author : Satoshi Horikoshi
ISBN : 9789811064661
Genre : Science
File Size : 74. 52 MB
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The principal aim of this book is to introduce chemists through a tutorial approach to the use of microwaves by examining several experiments of microwave chemistry and materials processing. It will subsequently enable chemists to fashion their own experiments in microwave chemistry or materials processing. Microwave heating has become a popular methodology in introducing thermal energy in chemical reactions and material processing in laboratory-scale experiments. Several research cases where microwave heating has been used in a wide range of fields have been reported, including organic synthesis, polymers, nanomaterials, biomaterials, and ceramic sintering, among others. In most cases, microwave equipment is used as a simple heat source. Therefore the principal benefits of microwave radiation have seldom been taken advantage of. One reason is the necessity to understand the nature of electromagnetism, microwave engineering, and thermodynamics. However, it is difficult for a chemist to appreciate these in a short time, so they act as barriers for the chemist who might take an interest in the use of microwave radiation. This book helps to overcome these barriers by using figures and diagrams instead of equations as much as possible.

Microwaves In Organic Synthesis

Author : Antonio de la Hoz
ISBN : 9783527651337
Genre : Science
File Size : 80. 75 MB
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The third edition of the bestselling two-volume reference covers everything you need to know about microwave technology for synthesis - from the best equipment to nonthermal effects, from solid-support reactions to catalysis. Completely revised and updated with half of the authors completely new to the project, this comprehensive work is clearly divided into two parts on the fundamentals of microwave irradiation, and application of microwaves and synergies with other enabling techniques. Also new to this edition are chapters on on-line monitoring, flow chemistry, combination with ultrasounds and natural products, including multicomponent reactions. An indispensable source for organic, catalytic, physical, and medicinal chemists.

Microwave Methods In Organic Synthesis

Author : Prasad Appukkuttan
ISBN : 9783540367574
Genre : Science
File Size : 47. 57 MB
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We are delighted to present this volume with contributions from some of the most renowned and experienced microwavechemists today. The delivery and introduction of energy has been closely connected with the discovery and investigation of new chemistry. It is with pleasure that we have seen an increased use of microwave irradiation over the years and we hope that this volume will re?ect the current interest in expanding the scopeofmicrowaveapplicationsinbothorganicandmedicinalchemistry. One important explanation behind the growth of microwave-enhanced chemistry has been the introductionof dedicated microwavereactors. As a result of this development we are proud to present a diverse set of - views. Apart fromchapters spanning the scope that is usually associated with microwavemethods, such as heterocyclic chemistry – an intriguing, but fr- tratingly diverse?eld that is excellently presented in one of the reviews – and transition metal-catalyzed reactions, we also present a review on microwa- assisted natural product chemistry, a topic that is of high interest and neither often nor widely covered. A contribution on microwave-accelerated synt- sis of protease inhibitors underlines the usefulness of microwave heating in medicinal chemistryandareview of?uorousmicrowavechemistryhighlights the importance of the combination of high-speed reactions and quick sepa- tions. Two separate chaptersonscaled-up microwavereactionsandgreen and sustainablechemistrygiveanoverviewofaspectsofmicrowavechemistrythat mightbeofgreatuseinbothindustrialandsmall-scaleapplications. We would like to take this opportunity to express our sincere gratitude to the contributors of this volume for their valuable time and efforts. We believe that the presented workwill further promotethe use of controlledmicrowave heating in both academia and industry.

Advances In Microwave Chemistry

Author : Bimal K Banik
ISBN : 9781351240482
Genre : Science
File Size : 56. 10 MB
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Advances in Microwave Chemistry discusses the novel bond formation methodologies, synergistic effects of microwaves with other entities, sample preparation including digestion, combustion, and extraction techniques, as well as selectivity in chemical processes. Recent updates are provided on microwave-assisted syntheses of pharmacologically significant aza-, oxo- and other heterocycles, including lactams, nucleosides, bile acids and sterols, the preparation of nanomaterials, composites, and absorber layer materials for thin film. This book also incorporates comparative discussions involving microwave irradiation with conventional methods in different aspects of organic, inorganic, medicinal, and green chemistry. Key Features: Provides a comparative discussion on microwave irradiation with conventional methods in different aspects of organic, inorganic, medicinal, and green chemistry Presents recent applications of microwave radiation in biocatalysis Offers a complete package correlating various aspects of microwaves in organic syntheses, the biological impact of products formed in reactions, pharmacological features, and environmental sustainability of the procedures Explains microwave-induced reactions on structurally complex bile acids and sterols Stands as a valuable and unique addition to the well-established book series, New Directions in Organic and Biological Chemistry

Green Chemistry

Author : Bela Torok
ISBN : 9780128095492
Genre : Science
File Size : 28. 48 MB
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Green Chemistry: An Inclusive Approach provides a broad overview of green chemistry for researchers from either an environmental science or chemistry background, starting at a more elementary level, incorporating more advanced concepts, and including more chemistry as the book progresses. Every chapter includes recent, state-of-the-art references, in particular, review articles, to introduce researchers to this field of interest and provide them with information that can be easily built upon. By bringing together experts in multiple subdisciplines of green chemistry, the editors have curated a single central resource for an introduction to the discipline as a whole. Topics include a broad array of research fields, including the chemistry of Earth’s atmosphere, water and soil, the synthesis of fine chemicals, and sections on pharmaceuticals, plastics, energy related issues (energy storage, fuel cells, solar, and wind energy conversion etc., greenhouse gases and their handling, chemical toxicology issues of everyday products (from perfumes to detergents or clothing), and environmental policy issues. Introduces the topic of green chemistry with an overview of key concepts Expands upon presented concepts with the latest research and applications, providing both the breadth and depth researchers need Includes a broad range of application based problems to make the content accessible for professional researchers and undergraduate and graduate students Authored by experts in a broad range of fields, providing insider information on the aspects or challenges of a given field that are most important and urgent

Microwave Chemistry

Author : Giancarlo Cravotto
ISBN : 9783110479935
Genre : Science
File Size : 52. 43 MB
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Microwave Chemistry has changed the way to work in chemical laboratories and is an established state-of-the-art technology to accelarate and enhance chemical processes. This book not only gives an overview of the technology, its historical development and theoretical background, but also presents its exceptionally broad spectrum of applications. Microwave Chemistry enables graduate students and scientist to learn and apply its methods successfully.

Microwave Assisted Cycloaddition Reactions

Author : Davor Margetic
ISBN : 1613241097
Genre : Technology & Engineering
File Size : 87. 60 MB
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The modern world imposes serious environmental challenges to chemists in reducing the human impact on nature. In this respect, organic reactions conducted in microwave conditions offer a 'green chemistry' method, which significantly enhances reaction efficiency, reduces the energy consumption, as well as the use of the toxic organic solvents. This book demonstrates the importance of the use of microwave technique in organic synthesis, in particular its application to cycloaddition reactions. In addition, this book offers a comprehensive overview of literature from the early accounts in the field of microwave assisted cycloadditions.

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